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In the presence of the guanidine HCl (at RT or below)–K[N(CN)(2)] mixtures a reaction which leads to the formation of N-iminoquinoxaline N-oxides takes place. N-Oxidation reaction is an additional postransformation of amino function in the 3-thiosemicarbazone compound. The reactions, according to the known mechanism, proceed according to the scheme of the Hofmann rearrangement. This is possible due to the participation of the guanidine fragments of the guanidine salt in the reaction. The iminoquinoxaline N-oxides are the products of the reaction. Reactions with dimethylformamide and N-chloroiminodiacetate lead to the alkylation of the 3-thiosemicarbazone fragments. Evidence for the existence of the oxazolidinone intermediate in the alkylation process is presented. The mechanism of the isomerization of N-iminoquinoxaline N-oxides to the iminoquinoxaline-N-oxide-imine derivatives and their irreversible transformation into quinoxaline-N-oxide-imine derivatives is discussed.Topic: Making Money Online

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